Solid-phase recrystallization of ZnS ceramics in phase transition region
Identifieur interne : 000B45 ( Russie/Analysis ); précédent : 000B44; suivant : 000B46Solid-phase recrystallization of ZnS ceramics in phase transition region
Auteurs : RBID : Pascal:01-0000727Descripteurs français
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Abstract
ZnS monocrystals, grown by solid-phase recrystallization (SPR) during hot pressing in the phase transition (PT) region are shown to have been improved by the doping of In. SPR of undoped and Al- or Ga-doped ZnS has not been successful. X-ray Laue patterns of as-grown ZnS monocrystal showed cubic symmetry. Scanning electron microscope investigation of the boundary surface between the monocrystalline and the polycrystalline parts of the as-grown ZnS:In ceramic disk showed an abnormal growth of crystallites into a monocrystal. To explain the role of In, high-temperature electrical conductivity (HTEC) measurements were performed. The temperature region from 1000°C to 500°C on the HTEC isobar of ZnS:In monocrystal was "cleared" from step-like PT changes, obligatorily observed on isobars of undoped and Cu-doped ZnS isobars in this region.
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<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Solid-phase recrystallization of ZnS ceramics in phase transition region</title>
<author><name sortKey="Lott, K" uniqKey="Lott K">K. Lott</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Tallinn Technical University, Ehitajate tee 5</s1>
<s2>Tallinn 19086</s2>
<s3>EST</s3>
<sZ>1 aut.</sZ>
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<country>Estonie</country>
<wicri:noRegion>Tallinn 19086</wicri:noRegion>
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<author><name sortKey="Anan Eva, G" uniqKey="Anan Eva G">G. Anan Eva</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>S.I. Vavilov State Optical Institute, All-Russia Scientific Center</s1>
<s2>193 171 St. Petersburg</s2>
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<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
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</affiliation>
</author>
<author><name sortKey="Gorokhova, E" uniqKey="Gorokhova E">E. Gorokhova</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>S.I. Vavilov State Optical Institute, All-Russia Scientific Center</s1>
<s2>193 171 St. Petersburg</s2>
<s3>RUS</s3>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
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<seriesStmt><idno type="ISSN">0022-0248</idno>
<title level="j" type="abbreviated">J. cryst. growth</title>
<title level="j" type="main">Journal of crystal growth</title>
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<profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Ceramics</term>
<term>Crystal doping</term>
<term>Experimental study</term>
<term>Grain growth</term>
<term>Growth from solid state</term>
<term>Heat treatments</term>
<term>Hot pressing</term>
<term>II-VI semiconductors</term>
<term>Impurity effect</term>
<term>Indium additions</term>
<term>Monocrystals</term>
<term>Recrystallization</term>
<term>Twinning</term>
<term>Zinc sulfides</term>
</keywords>
<keywords scheme="Pascal" xml:lang="fr"><term>Etude expérimentale</term>
<term>Recristallisation</term>
<term>Méthode état solide</term>
<term>Traitement thermique</term>
<term>Pressage chaud</term>
<term>Monocristal</term>
<term>Semiconducteur II-VI</term>
<term>Zinc sulfure</term>
<term>Dopage cristal</term>
<term>Addition indium</term>
<term>Croissance grain</term>
<term>Effet impureté</term>
<term>Maclage</term>
<term>Céramique</term>
<term>8110J</term>
<term>ZnS:In</term>
<term>S Zn</term>
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<front><div type="abstract" xml:lang="en">ZnS monocrystals, grown by solid-phase recrystallization (SPR) during hot pressing in the phase transition (PT) region are shown to have been improved by the doping of In. SPR of undoped and Al- or Ga-doped ZnS has not been successful. X-ray Laue patterns of as-grown ZnS monocrystal showed cubic symmetry. Scanning electron microscope investigation of the boundary surface between the monocrystalline and the polycrystalline parts of the as-grown ZnS:In ceramic disk showed an abnormal growth of crystallites into a monocrystal. To explain the role of In, high-temperature electrical conductivity (HTEC) measurements were performed. The temperature region from 1000°C to 500°C on the HTEC isobar of ZnS:In monocrystal was "cleared" from step-like PT changes, obligatorily observed on isobars of undoped and Cu-doped ZnS isobars in this region.</div>
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<fA15 i1="02"><s1>Sony Corp.</s1>
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<fC01 i1="01" l="ENG"><s0>ZnS monocrystals, grown by solid-phase recrystallization (SPR) during hot pressing in the phase transition (PT) region are shown to have been improved by the doping of In. SPR of undoped and Al- or Ga-doped ZnS has not been successful. X-ray Laue patterns of as-grown ZnS monocrystal showed cubic symmetry. Scanning electron microscope investigation of the boundary surface between the monocrystalline and the polycrystalline parts of the as-grown ZnS:In ceramic disk showed an abnormal growth of crystallites into a monocrystal. To explain the role of In, high-temperature electrical conductivity (HTEC) measurements were performed. The temperature region from 1000°C to 500°C on the HTEC isobar of ZnS:In monocrystal was "cleared" from step-like PT changes, obligatorily observed on isobars of undoped and Cu-doped ZnS isobars in this region.</s0>
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<pR><fA30 i1="01" i2="1" l="ENG"><s1>International Conference on II-VI Compounds</s1>
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